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Synthesis and structure of cot-Pt(II) complexes 송아란, 하 광*

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Theories and Applications of Chem. Eng., 2007, Vol. 13, No. 2 2560

화학공학의 이론과 응용 제13권 제2호 2007년

Synthesis and structure of cot-Pt(II) complexes 송아란, 하 광

*

전남대학교 응용화학공학과

([email protected]*)

[(cot)PtX2](cot=(1,2,5,6-η)-1,3,5,7-cyclooctatetraene, X=Cl, I) was synthesized from a starting material, K2PtCl4. The reaction of alkyl or aryl Grignard reagents with [(cot)PtX2] yields a series of products which are the type of [(cot)PtR2] or [R2Pt(cot)PtR2](R=CH3, C6H5). An improved synthesis for [(cot)PtX2] complexes and the reaction with HI to give [(cot)PtRI] are described. The reaction of [(cot)PtR2](R=CH3) with K2PtCl4 yields cyclooctatetraene-Platinum dimer, [Cl2Pt(cot)PtR2]. The method of synthesis and formation mechanism of this series of compounds are introduced, the spectral data are discussed, and structure of this compounds are proposed.

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