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Transmission Electron Microscopy Characterization of Early Pre-Transition Oxides Formed on ZIRLO

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Table  1.  Nominal  chemical  composition  of  ZIRLO TM   tube  samples investigated  in  this  work
Fig.  2.  (a)  Dark-field  TEM  image  of  300-hour  sample  showing  the  faint  area  at  the  metal/oxide  interface  (b)  EDS  line  profile  data  of  (c)  Dark-field  TEM  image  of  300-hour  sample  showing  the  clear  metal/  oxide  interface  (d
Fig.  4.  (a)  Average  oxide  thickness  on  the  300-hour  sample  and  under  three  types  of  lateral  crack  (b)  Average  oxide  thickness  on  the  50-day  sample  and  under  three  types  of  lateral  cracks.
Fig.  5.  (a)  High  resolution  TEM  images  of  300-hour  sample  showing  equiaxed  oxide  grains  and  some  interlinked  voids  at  the  water/oxide  interface  (b)  STEM  image  of  outer  oxide  formed  on  50-day  sample.
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