Analysis of Residual Fatty Acid of the Fish Bone Excavated from Bupchon-ri in Wonju(II)

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(1)Conservation Science in Museum Vol. 2, pp. 51~55(2000).

(2) (II) †.

(3) Analysis of Residual Fatty Acid of the Fish Bone Excavated from Bupchon-ri in Wonju(II) Hei-sun Yu† and Young-ju Jeong Conservation Science Lab., The National Museum of Korea.

(4) (4 ) ! 26 " #$ %&'() *+, -./01. 2 *$ 43 (45, 67, 89, :7) #$ %& '() *+ 58;<=> ?@/A 7 /BC /01. *+D EFGHIJKL(Gas chromato -graphy) <M/A '(), *N/0B, O O3 PQ, R)/A .ST '() *UVW, /01. ' ()*U ;<=3 X+, YX Z[\]^ _`**+a, <M/01. Abstract This study is an analysis of residual fatty acid of the unidentified 26 fish bone samples which were excavated from Bupchon-ri in Wonju, Kangwon province. The purpose of this study is to identify fish kind by comparing the residual fatty acid analysis with the reference data of croaker, shark, herring and weakfish. Fatty acid was separated by gas chromatography and distribution pattern was analyzed by calculating composition of each sample. Principal component analysis(PCA), one of multivariate analysis method was used to understand fatty acid distribution data.. I.. . ts) => DEF uvw ) xy z{|} P ~L$ - 4) M'(+, ;, , ;F) GHIJK-. T 0 ~ 67 . 5a => DEF) GH IJK-. NOP + L$ P a DE F 26 M' RT5 T7. * => DEFa 55L$ g ) `P 6a $ BC AP I C ,¡5, ¢\L$ -. N]a £# %& '() DEF ¤¥¦ N]^_$ L$ § GHIJK -.[\¨ ©ª ) M' «¬TaN ®|}$ /¯° ±L$ ²³ 7. .C A_´$µ>g¶(Gas chromatography)P ¯ T IJK -T5, · ·) ¸¹ ºKT b).

(5) 90 !" #$ % & '() *+, -. /01 2345 67. 89 :; <1 =>?@A BC DEF GHIJK -.L$ 5 ) M' .NOP Q RSTU 4VLW, XYZ' IJK-. [\P N]^_`Ta b cdP ef 5 67. g h$ ijk jlm nop qrs(4 a). 1). 5). 2-4). †. Corresponding author : Hei-sun Yu, Conservation Science Lab., The National Museum of Korea Tel : 02) 398-5146 Fax : 02) 398-5130 E-mail : [email protected]. (Residual fatty acid analysis)

(6) ! " #$ %&'( )# *+ ,- ./0 123 4567 . b) 89:;: <=> ?@(AB CDE>). a). https://doi.org/10.22790/conservation.2000.2.0051. 51.

(7) 2 (2000). 52. » IJK -¼½¾ RT7. IJK -¼N O) ¿. À¿ %ÁÂ( ÃÄ--. (Principal component analysis) ¯T7. 6). II.. . ijk jlm nop qrs(4ts) => DEF ÅÆÇ» ÈAÉT ÊRTU P a DEF 26 GHIJK -. T 7. -. Ë¯ <Ì Table 1 OÍV7. 2. ÎR DEF -.CÏqr 4ts D EF (I)Ð\ ÑÒ Ó T7. IJK ©Ô -¼ N] ¿.\ ÑÕ À¿ %ÁÂ( ÃÄ--.(PCA) ¯T7. 1.. 5). III.. . 4Ö- => ÎR DEF 26) ;R ÀT GHIJK -. T5, · ©ÔN] ×Ø ÀT 7Ù- Ã Ä--.(PCA) T7. 1.

(8) (40) PCA · ©ÔN] ×Ø ÀT 7Ù- ÃÄ--. [\ Ú 4" gÚ[2") +F (Û)gÚ, ;F(Ü)gÚ ¼©T5 6a F (Ý )gÚ, ;F(Þ )gÚ]L$ ß-§ 6V7(Fig. 1). À) - [\P +à$ T ÎR ;) -. T7. 2.

(9) (40) + (26) PCA => DEF 40) GHIJK -.. Table 1. Characteristics of analytical samples Serial no.. Sample no.. Sample (g). Total lipid (mg). Extraction efficiency (%). 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26. 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66. 30.2020 40.8870 19.0235 35.7141 4.7776 7.0640 133.1078 12.7423 20.7343 25.3081 10.4144 20.1101 17.6551 19.9270 48.5701 80.3382 10.9366 2.5532 15.0004 3.7819 5.2828 33.5666 7.7418 10.6591 27.7934 7.1558. 2.8 4.3 1.9 5.1 0.8 0.6 3.4 1.0 2.0 0.9 0.5 0.9 3.6 0.6 2.0 3.2 0.2 0.5 2.2 1.8 2.0 3.5 3.3 1.5 1.6 0.6. 0.0927 0.0105 0.0100 0.0143 0.0017 0.0085 0.0026 0.0078 0.0096 0.0045 0.0048 0.0045 0.0204 0.0030 0.0041 0.0040 0.0018 0.0196 0.0147 0.0476 0.0379 0.0104 0.0426 0.0141 0.0058 0.0084. Remark. (*no. 9) ? ?. (no. 10) ?. (no. 28) (no. 7) (no. 12) (no. 13) . (no. 20) ?

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(14) (II). 53. Fig. 1. PCA result for reference samples from Bupchon-ri site.. Fig. 2. PCA result for reference samples and unidentified samples from Bupchon-ri site.. NO¨ P a DEF 26) GHI JK -.NO ÃÄ--. [\ ´ U 4" gÚ[+F(Û)gÚ, ;F(Ü)gÚ ¼©T5 6a F(Ý )gÚ, ;F(Þ )gÚ, ÎR DEF (á)gÚ]L$ ß-§ 6V7(Fig. 2). <1 no.. ) â F gÚ Í ¼©45 6a ± L$ Fã 6V7. gä å-) ÎR DEFa æÒ;L$ - DEF) gÚ\ a 7ç »") gÚ èÄT5 6a ± é 6 7. ê, æÒ; ëì 2 ) DE íî 45, 46, 58.

(15) 54. 2 (2000). Fig. 3. PCA result for unidentified samples from Bupchon-ri site.. L$ HïT5 6a ±L$ ðÕ 7. íî;) P ÀT ÎR DEF PCA-. [\$ · ) -¼Õ@P ñòTLW, g [\a ëó 3\ ô7. 3. (26) ÎR DEF) GHIJK -.NO ÃÄ --. [\ Ú 5" gÚ[Û, Ý , Þ , Ü, ágÚ]L$ ÊRTU -4a ± 6V7(Fig. 3). ê, 2 $ - no. 45, 46, 58 T ) gÚ(Ý ) èÄT5 65, õI gÚ:C fA I ) ; öî4; 6 ±L$ ðÕ4V7. ö î4; 6a ; ðÕT+ ÀT DEF) I JKNO PCA[\(Fig. 1)P ÷5$ T7. ÎR DEFa æÒ; E»T5 øë 6ù Fú$ NO¨ b ûü 6 ±L$ ð ý 7. gäú$ öî; RT+ ÀT þÿ E » DEF ) P RT5, DE F) - [\¨ TLW, g [\a Table 2 OÍV7. +¨ FP E»T5 øC F no. 55, 56 ôC gÚ(Ü) èÄT5 6LW, +FP E» T5 øC F no. 47, 48, 49¨ FP E»T5 øC F no. 50, +¨ ;FP E»T5 øC F no. 53, +¨ ;FP E»T5 øC F no. 65, 66 T ) gÚ(Û) èÄT5 67. +FP E»T5. Table 2. PCA result for unidentified fish bone samples Mark. + , . /. Sample no.. Certified fish. 45, 46, 58 41, 43, 44, 51, 63, 64 47, 48, 49, 50, 53, 65, 66. Herring Croaker+Herring+Weakfish Croaker+Herring+Weakfish +Shark 42, 52, 54, 57, 59, 60, 61, 62 Shark+Herring+Weakfish 55, 56 Croaker+Herring. øC F no. 41, 44, +¨ FP E»T5 øC F no. 63, +¨ ;FP E»T5 øC F no. 64A ô C gÚ(á) èÄT5, ;FP E»T5 øC F no. 52, ¨ ;FP E»T5 øC F no. 59, ¨ ;FP E»T5 øC F no. 62A ôC gÚ(Þ ) èÄT5 67. ) [\P S ÎR DEF 26 3) ; R§ 6VLW, ðÕ [\ T I öî ; -+ 6a 9 eP µü 7a N b ))A 67. Ã * => DEF 1

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(19). 012, 345, 67 89 :;< => ?", @ABCD:, Vol. 4, No. 1 (1995) 2. EFG, 012, 345, H?I<JKL MN O= >", PQRS, 9, pp.159-180, TUPQVWXYZ 1.. 55. 345,[\]^_ àJ bcdef !", g7h@ABC, ij*, pp.53-59 (1999) 4. 345, 012, klmn,op qrJ 3*= s tu !", vwx yz 3 (= >){, pp.116-129, |}~ (2001 ) 5. 345, , 4 !(I)", v(I) Q{ , |}g7h (2000) 6. : , f C '(f =", C C g#C¡ ¢~ (1989) (1998). 3..

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